Antioxidant 1076 synthesis
- Product Name:Antioxidant 1076
- CAS Number:2082-79-3
- Molecular formula:C35H62O3
- Molecular Weight:530.86
112-92-5
481 suppliers
$5.00/10g
6386-38-5
173 suppliers
$13.00/10g
2082-79-3
390 suppliers
$6.00/10g
Yield:2082-79-3 99.1%
Reaction Conditions:
with sodium montmorillonite in methanol at 110 - 120; under 15001.5 - 22502.3 Torr; for 7 h;Inert atmosphere;Reagent/catalyst;
Steps:
4
584 g of methyl β-(3,5-di-tert-butyl-4-hydroxyphenyl)propionate, 541 g octadecanol, 0.58gSodium montmorillonite, 100 ml of methanol was added to the flask with mechanical stirring, Thermometer socket,In a 2000 ml four-necked flask equipped with a stirrer,Heating the material with a heating jacket,And stirring is started,Temperature reached 110-120 ,Filled with nitrogen, So that the reaction system pressure control in 2-3MPa, 7h after the end of the reaction,Cooled to 20 ° C,filter,drying, octadecanol β-(3,5-di-tert-butyl-4-hydroxyphenyl)propionate.
References:
CN106278880,2017,A Location in patent:Paragraph 0017-0028
112-92-5
481 suppliers
$5.00/10g
20170-32-5
157 suppliers
$13.00/5g
2082-79-3
390 suppliers
$6.00/10g
112-92-5
481 suppliers
$5.00/10g
2082-79-3
390 suppliers
$6.00/10g
112-92-5
481 suppliers
$5.00/10g
818-08-6
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$14.00/25G
6386-38-5
173 suppliers
$13.00/10g
2082-79-3
390 suppliers
$6.00/10g