Methyl 4-{[(tert-butoxy)carbonyl]amino}-3-methoxybenzoate synthesis
- Product Name:Methyl 4-{[(tert-butoxy)carbonyl]amino}-3-methoxybenzoate
- CAS Number:941715-64-6
- Molecular formula:C14H19NO5
- Molecular Weight:281.3
![Benzoic acid, 4-[[(1,1-dimethylethoxy)carbonyl]amino]-3-hydroxy-, methyl ester](/CAS/20210305/GIF/941715-62-4.gif)
Yield:941715-64-6 86%
Reaction Conditions:
Stage #1: methyl 4-(t-butoxycarbonylamino)-3-hydroxybenzoatewith sodium hydride in N,N-dimethyl-formamide at 20; for 0.5 h;
Stage #2: methyl iodide in N,N-dimethyl-formamide; for 1 h;Further stages.;
References:
Ahn, Jung-Mo;Han, Sun-Young [Tetrahedron Letters,2007,vol. 48,# 20,p. 3543 - 3547]
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