[2-(4,4,5,5-Tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenoxy]-acetonitrile synthesis
- Product Name:[2-(4,4,5,5-Tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenoxy]-acetonitrile
- CAS Number:936250-19-0
- Molecular formula:C14H18BNO3
- Molecular Weight:259.11
533-58-4
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936250-19-0
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Yield:-
Steps:
Multi-step reaction with 2 steps
1: potassium carbonate; 18-crown-6 ether / acetone / 1 h / 55 °C / Microwave irradiation
2: triethylamine; palladium diacetate; CyJohnPhos / 1,4-dioxane / 1.5 h / 100 °C / Inert atmosphere
References:
Manasieva, Leda Ivanova;Maria, Battisti Umberto;Prandi, Adolfo;Brasili, Livio;Franchini, Silvia [Synthesis,2015,vol. 47,# 23,art. no. SS-2015-T0293-OP,p. 3767 - 3775]