4-CHLOROMETHYL-2-(3,4-DIMETHOXY-PHENYL)-5-METHYL-OXAZOLE synthesis
- Product Name:4-CHLOROMETHYL-2-(3,4-DIMETHOXY-PHENYL)-5-METHYL-OXAZOLE
- CAS Number:907200-66-2
- Molecular formula:C13H14ClNO3
- Molecular Weight:267.71
120-14-9
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907200-66-2
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Yield:-
Steps:
Multi-step reaction with 2 steps
1: hydrogenchloride / glacial acetic acid; 1,4-dioxane / 16 h / 0 - 20 °C
2: trichlorophosphate / 1,2-dichloro-ethane / 0.5 h / Reflux
References:
He, Shanshan;Li, Kelin;Lin, Billy;Hu, Zongyi;Xiao, Jingbo;Hu, Xin;Wang, Amy Q.;Xu, Xin;Ferrer, Marc;Southall, Noel;Zheng, Wei;Aubé, Jeffrey;Schoenen, Frank J.;Marugan, Juan J.;Liang, T. Jake;Frankowski, Kevin J. [Journal of Medicinal Chemistry,2017,vol. 60,# 14,p. 6364 - 6383]