9-Bromo-10-(2-naphthyl)anthracene synthesis
- Product Name:9-Bromo-10-(2-naphthyl)anthracene
- CAS Number:474688-73-8
- Molecular formula:C24H15Br
- Molecular Weight:383.28
128-08-5
847 suppliers
$5.00/5G
7424-72-8
54 suppliers
$75.00/100mg
474688-73-8
227 suppliers
$15.00/1g
Yield:474688-73-8 99%
Reaction Conditions:
in water;N,N-dimethyl-formamide;
Steps:
S.5 Synthesis Example 5
Synthesis Example 5 (Synthesis of 9-bromo-10-(naphthalene-2-yl)anthracene) 23.1 g of 9-(naphthalene-2-yl)anthracene was dispersed into 250 ml of DMF (dimethylformamide), and then 14.9 g of NBS (N-bromosuccinimide) in DMF solution (150 ml) was dropped therein. After stirred at room temperature for 7 hours, it was left over a night. 200 ml of water was added thereto, and then the crystal precipitated was separated by filtration. Subsequently it was washed by ethanol adequately, followed by drying, and 28.8 g of 9-bromo-10-(naphthalene-2-yl)anthracene of beige color crystal was obtained (Yield: 99%).
References:
US2007/152565,2007,A1
523-27-3
390 suppliers
$6.00/5g
32316-92-0
477 suppliers
$6.00/1g
474688-73-8
227 suppliers
$15.00/1g
7424-72-8
54 suppliers
$75.00/100mg
474688-73-8
227 suppliers
$15.00/1g
580-13-2
502 suppliers
$6.00/1g
474688-73-8
227 suppliers
$15.00/1g
32316-92-0
477 suppliers
$6.00/1g
474688-73-8
227 suppliers
$15.00/1g