5-FLUORO-1-TRIISOPROPYLSILANYL-1H-PYRROLO[2,3-B]PYRIDINE synthesis
- Product Name:5-FLUORO-1-TRIISOPROPYLSILANYL-1H-PYRROLO[2,3-B]PYRIDINE
- CAS Number:868387-37-5
- Molecular formula:C16H25FN2Si
- Molecular Weight:292.47
![5-BROMO-1-TRIISOPROPYLSILANYL-1H-PYRROLO[2,3-B]PYRIDINE](/CAS/GIF/858116-66-2.gif)
858116-66-2
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$55.00/250mg
868387-37-5
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$150.00/25mg
Yield:868387-37-5 63%
Reaction Conditions:
Stage #1: 5-bromo-1-(triisopropylsilyl)-1H-pyrrolo[2,3-b]pyridinewith n-butyllithium in tetrahydrofuran at -78; for 1 h;Inert atmosphere;
Stage #2: with N-fluorobis(benzenesulfon)imide in tetrahydrofuran at -78 - 20; for 2 h;
References:
WO2017/133667,2017,A1 Location in patent:Page/Page column 106; 107
858116-66-2
72 suppliers
$55.00/250mg
![1-[Tris(1-methylethyl)silyl]-1H-pyrrolo[2,3-b]pyridine](/CAS/20180601/GIF/1093759-49-9.gif)
1093759-49-9
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868387-37-5
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$150.00/25mg
![5-FLUORO-1H-PYRROLO[2,3-B]PYRIDINE](/CAS/GIF/866319-00-8.gif)
866319-00-8
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13154-24-0
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$20.00/10g
868387-37-5
23 suppliers
$150.00/25mg
13154-24-0
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183208-35-7
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$5.00/1g
868387-37-5
23 suppliers
$150.00/25mg