BZ-DMT-DEOXYADENOSINE 2-CLPH DIESTER TRIETHYLAMMONIUM SALT synthesis
- Product Name:BZ-DMT-DEOXYADENOSINE 2-CLPH DIESTER TRIETHYLAMMONIUM SALT
- CAS Number:85381-22-2
- Molecular formula:C50H54ClN6O9P
- Molecular Weight:949.44
15715-58-9
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64325-78-6
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$9.00/250mg
15074-54-1
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$19.00/1g
85381-22-2
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Yield:-
Reaction Conditions:
Stage #1: N6-benzoyl-5'-O-(4,4'-dimethoxytrityl)-2'-deoxyadenosine;2-chlorophenyl dichlorophosphatewith pyridine;1,2,3-triazole in dichloromethane at 0; for 2.5 h;
Stage #2: triethylamine carbonatewith water in dichloromethane;Further stages.;
References:
Yagodkin, Andrey;Azhayev, Alex;Roivainen, Jarkko;Antopolsky, Maxim;Kayushin, Alexei;Korosteleva, Maria;Miroshnikov, Anatoly;Randolph, John;Mackie, Hugh [Nucleosides, nucleotides and nucleic acids,2007,vol. 26,# 5,p. 473 - 497]