1-[1-[2-(2,4-Dinitrophenyl)hydrazono]ethyl]cyclopropane synthesis
1synthesis methods
- Product Name:1-[1-[2-(2,4-Dinitrophenyl)hydrazono]ethyl]cyclopropane
- CAS Number:790-13-6
- Molecular formula:
- Molecular Weight:0
Yield:790-13-6 59%
Reaction Conditions:
with acetic acid in ethanol; for 10 h;Reflux;
Steps:
Synthesis of 4-nitro- and 2,4-dinitrophenylhydrazones
General procedure: A mixture of arylhydrazine (5mmol), ketone (6 mmol) and AcOH (0.5 mL) in EtOH (20 mL) was heated to refluxfor the time indicated below. The product was purified by recrystallizationfrom ethanol.
References:
Salikov, Rinat F.;Belyy, Aleksandr Yu.;Tomilov, Yury V. [Tetrahedron Letters,2014,vol. 55,# 43,p. 5936 - 5939] Location in patent:supporting information