9ALPHA,11ALPHA-METHYLENE-15S-HYDROXY-11A-DEOXY-11A-METHYLENE-THROMBA-5Z,13E-DIEN-1-OIC ACID synthesis
- Product Name:9ALPHA,11ALPHA-METHYLENE-15S-HYDROXY-11A-DEOXY-11A-METHYLENE-THROMBA-5Z,13E-DIEN-1-OIC ACID
- CAS Number:74034-56-3
- Molecular formula:C22H36O3
- Molecular Weight:348.52
17814-85-6
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74034-56-3
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Yield:-
Steps:
Multi-step reaction with 4 steps
1: dimsyl sodium / dimethylsulfoxide / 25 °C
2: 74 percent / dimethylsulfoxide / 1 h
3: 65 percent / H2O / acetic acid; trifluoroacetic acid / 10 h / 45 °C
4: 95 percent / 1N LiOH / tetrahydrofuran; H2O / 12 h / Ambient temperature
References:
Nicolaou;Magolda;Claremon [Journal of the American Chemical Society,1980,vol. 102,# 4,p. 1404 - 1409]
39968-97-3
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74034-56-3
22 suppliers
$45.00/100μg