7-Aminopyrazolo[1,5-a]pyrimidine-6-carbonitrile synthesis
- Product Name:7-Aminopyrazolo[1,5-a]pyrimidine-6-carbonitrile
- CAS Number:89975-57-5
- Molecular formula:C7H5N5
- Molecular Weight:159.15
1225387-53-0
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123-06-8
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$14.14/1gm:
89975-57-5
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Yield:89975-57-5 90 %
Reaction Conditions:
with pyridineReflux;
Steps:
General procedure for the synthesis of 7-aminoazolo[1,5-a]pyrimidine-6-carbonitriles 3a-3w
General procedure: A mixture of 0.01 mol of appropriate aminoazole 1a-1w, 0.01 mol (1.22 g) of (ethoxymethylidene)malononitrile 2, and 25 mL of pyridine was heated under reflux (3l was prepared at 70°C) for 1-7 h (specific time is noted for each reaction). The reaction mixture was cooled to ambient temperature, target product was isolated by procedure noted below.
References:
Urakov;Savateev;Rusinov [Doklady Chemistry,2022,vol. 505,# 2,p. 168 - 176][Dokl. Akad. Nauk,2022,vol. 505,p. 40 - 49]
1820-80-0
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$5.00/5g
16849-88-0
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$100.00/500mg
89975-57-5
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102781-32-8
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89975-57-5
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