[[[(2R,3S,4R,5R)-5-(2-amino-6-oxo-3H-purin-9-yl)-3,4-dihydroxyoxolan-2-yl]methoxy-hydroxyphosphoryl]oxy-hydroxyphosphoryl] [(2R,3S,4R,5R)-5-(2-amino-6-oxo-3H-purin-9-yl)-3,4-dihydroxyoxolan-2-yl]methyl hydrogen phosphate synthesis

1synthesis methods

Product Name:[[[(2R,3S,4R,5R)-5-(2-amino-6-oxo-3H-purin-9-yl)-3,4-dihydroxyoxolan-2-yl]methoxy-hydroxyphosphoryl]oxy-hydroxyphosphoryl] [(2R,3S,4R,5R)-5-(2-amino-6-oxo-3H-purin-9-yl)-3,4-dihydroxyoxolan-2-yl]methyl hydrogen phosphate
CAS Number:6674-45-9
Molecular formula:C20H27N10O18P3
Molecular Weight:788.41

85-32-5 Synthesis

85-32-5
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[[[(2R,3S,4R,5R)-5-(2-amino-6-oxo-3H-purin-9-yl)-3,4-dihydroxyoxolan-2-yl]methoxy-hydroxyphosphoryl]oxy-hydroxyphosphoryl] [(2R,3S,4R,5R)-5-(2-amino-6-oxo-3H-purin-9-yl)-3,4-dihydroxyoxolan-2-yl]methyl hydrogen phosphate

6674-45-9
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146-91-8 Synthesis

146-91-8
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[[(2R,3S,4R,5R)-5-(2-amino-6-oxo-3H-purin-9-yl)-3,4-dihydroxyoxolan-2-yl]methoxy-hydroxyphosphoryl] [(2R,3S,4R,5R)-5-(2-amino-6-oxo-3H-purin-9-yl)-3,4-dihydroxyoxolan-2-yl]methyl hydrogen phosphate

34692-44-9
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Yield:6674-45-9 71%

Reaction Conditions:

with pyridine;1-methyl-pyrrolidin-2-one;N,N,N,N,N,N-hexamethylphosphoric triamide;tributyl-amine;S,S'-bis(4-chlorophenyl) phosphorodithioate;silver nitrate at 0 - 20; for 7 h;

References:

Fukuoka, Koichiro;Suda, Fuminori;Suzuki, Ryo;Ishikawa, Masahide;Hata, Tsujiaki [Chemistry Letters,1994,# 3,p. 499 - 502]