2-(N-acetylacetamido)-3-(4-hydroxy-3-methoxyphenyl)propanoic acid synthesis
- Product Name:2-(N-acetylacetamido)-3-(4-hydroxy-3-methoxyphenyl)propanoic acid
- CAS Number:63357-45-9
- Molecular formula:C12H15NO5
- Molecular Weight:253.25
![Benzene, 4-(bromomethyl)-1-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-2-methoxy-](/CAS/20210305/GIF/113931-97-8.gif)
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Yield:-
Steps:
Multi-step reaction with 3 steps
1.1: sodium hydride / mineral oil; N,N-dimethyl-formamide / 0.17 h / 0 °C / Inert atmosphere
1.2: 4 h / 0 °C / Inert atmosphere
2.1: potassium hydroxide / water; ethanol / 3 h / Inert atmosphere; Reflux
3.1: hydrogenchloride / water / 6 h / Reflux
References:
Schneider, Tobias;Kubyshkin, Vladimir;Budisa, Nediljko [European Journal of Organic Chemistry,2018,vol. 2018,# 18,p. 2053 - 2063]
![Benzaldehyde, 4-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-3-methoxy-](/CAS/20180601/GIF/69404-94-0.gif)
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![[4-[tert-butyl(dimethyl)silyl]oxy-3-methoxyphenyl]methanol](/CAS/20180601/GIF/113931-96-7.gif)
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139-85-5
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121-33-5
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