2,3-(4-CARBOXYBENZO)-1,4,7,10,13,16-HEXAOXACYCLOOCTADEC-2-ENE synthesis
- Product Name:2,3-(4-CARBOXYBENZO)-1,4,7,10,13,16-HEXAOXACYCLOOCTADEC-2-ENE
- CAS Number:60835-75-8
- Molecular formula:C17H24O8
- Molecular Weight:356.37
14098-24-9
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$42.00/1g
76-05-1
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$9.00/1g
60835-75-8
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$28.00/5MG
Yield:60835-75-8 70%
Reaction Conditions:
Stage #1:2,3,5,6,8,9,11,12,14,15-decahydro-1,4,7,10,13,16-benzohexaoxacyclooctadecin;trifluoroacetic acid with hexamethylenetetramine for 24.3333 h;Reflux;Inert atmosphere;Cooling with ice;
Stage #2: with hydrogenchloride for 2.5 h;Inert atmosphere;Cooling with ice;
References:
Shao, Shuai;Thomas, Michael B.;Park, Kyu Hyung;Mahaffey, Zoe;Kim, Dongho;D'Souza, Francis [Chemical Communications,2017,vol. 54,# 1,p. 54 - 57] Location in patent:supporting information