6-Methoxy-2,4-dihydro-1,4-benzothiazin-3-one synthesis

3synthesis methods

Product Name:6-Methoxy-2,4-dihydro-1,4-benzothiazin-3-one
CAS Number:99286-44-9
Molecular formula:C9H9NO2S
Molecular Weight:195.24

Acetic acid, 2-[(4-methoxy-2-nitrophenyl)thio]-, ethyl ester

100638-07-1
0 suppliers
inquiry

6-Methoxy-2,4-dihydro-1,4-benzothiazin-3-one

99286-44-9
21 suppliers
$150.00/250mg

Yield:99286-44-9 93%

Reaction Conditions:

with iron;acetic acid at 90; for 3 h;

References:

Reck, Folkert;Alm, Richard;Brassil, Patrick;Newman, Joseph;Dejonge, Boudewijn;Eyermann, Charles J.;Breault, Gloria;Breen, John;Comita-Prevoir, Janelle;Cronin, Mark;Davis, Hajnalka;Ehmann, David;Galullo, Vincent;Geng, Bolin;Grebe, Tyler;Morningstar, Marshall;Walker, Phil;Hayter, Barry;Fisher, Stewart [Journal of Medicinal Chemistry,2011,vol. 54,# 22,p. 7834 - 7847] Location in patent:experimental part

2365-48-2 Synthesis

2365-48-2
352 suppliers
$19.00/25g

153898-63-6
98 suppliers
$19.00/250mg

99286-44-9
21 suppliers
$150.00/250mg

References

14482-32-7
11 suppliers
inquiry

79-11-8
10 suppliers
$27.00/25g

99286-44-9
21 suppliers
$150.00/250mg

References