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ChemicalBook CAS DataBase List 6-Bromoisatinic anhydride
77603-45-3

6-Bromoisatinic anhydride synthesis

10synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 5 steps
1: 92 percent / stannous chloride dihydrate / ethanol / Heating
2: 77 percent / 0.17 h
3: 73 percent / MgSO4*7H2O; KMnO4 / H2O / 2 h / Heating
4: aq. HCl / 48 h / 55 - 60 °C
5: 92 percent / NaOH / H2O; toluene / 0.25 h / 0 °C

References:

Katsifis, Andrew G.;McPhee, Meredith E.;Mattner, Filomena;Ridley, Damon D. [Australian Journal of Chemistry,1999,vol. 52,# 11,p. 1061 - 1069]

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