5-PHENYL-FURAN-2-CARBONYL CHLORIDE synthesis
- Product Name:5-PHENYL-FURAN-2-CARBONYL CHLORIDE
- CAS Number:57489-93-7
- Molecular formula:C11H7ClO2
- Molecular Weight:206.63
52938-97-3
84 suppliers
$45.00/10mg
57489-93-7
19 suppliers
$81.37/1g
Yield:57489-93-7 100%
Reaction Conditions:
with thionyl chloride in toluene at 70; for 4 h;Product distribution / selectivity;
Steps:
1b
Example lb: 5-phenylfuran-2-carbonyl chloride5-phenylfuran-2-carboxylic acid (15.00 g, 79.71 mmol) was suspended in thionyl chloride (30 mL) and heated at 70°C for 4h. The reaction mixture was dried under vacuum at 60°C to give a light green solid in quantitative yield. This material was used in the next step without further purification.
References:
WO2011/159781,2011,A2 Location in patent:Page/Page column 55
52938-97-3
84 suppliers
$45.00/10mg
79-37-8
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$17.67/10gm:
57489-93-7
19 suppliers
$81.37/1g
88-14-2
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$5.00/10g
57489-93-7
19 suppliers
$81.37/1g
62-53-3
660 suppliers
$10.00/1g
57489-93-7
19 suppliers
$81.37/1g
2527-99-3
191 suppliers
$6.00/1g
57489-93-7
19 suppliers
$81.37/1g