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ChemicalBook CAS DataBase List 5-methyl-5-propyl-1,3-dioxan-2-one
7148-50-7

5-methyl-5-propyl-1,3-dioxan-2-one synthesis

5synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: p-toluenesulfonyl chloride; n-butyllithium
1.2: 0 - 60 °C
2.1: C49H74AlNO4; bis(triphenylphosphoranylidene)ammonium iodide / butanone / 24 h / 110 °C / 7500.75 Torr / Autoclave; Sealed tube

References:

Guo, Wusheng;Laserna, Victor;Rintjema, Jeroen;Kleij, Arjan W. [Advanced Synthesis and Catalysis,2016,vol. 358,# 10,p. 1602 - 1607]

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