5-Methyl-4-hexenoic acid methyl ester synthesis

10synthesis methods

Product Name:5-Methyl-4-hexenoic acid methyl ester
CAS Number:35901-76-9
Molecular formula:
Molecular Weight:0

1445-45-0 Synthesis

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115-18-4
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802294-64-0 Synthesis

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Yield:35901-76-9 98%

Reaction Conditions:

at 125; for 12 h;

Steps:

i Example i

Synthesis of compound I-1. In the flask, add trimethyl orthoacetate (1 mol), 2-methyl-3-buten-2-ol (1 mol) and propionic acid (0.2 mol), then heat the reaction system to 125°C, and continue to stir the reaction 12h, the reaction was stopped.Washed with water, saturated NaHCO₃and saturated brine successively, dried over anhydrous sodium sulfate, and distilled under reduced pressure at 30 hPa and 70 °C to obtain compound I (yield 98%).

References:

CN114315497,2022,A Location in patent:Paragraph 0048-0051

1445-45-0 Synthesis

1445-45-0
344 suppliers
$10.00/5mL

115-18-4
182 suppliers
$10.00/5g

35901-76-9
0 suppliers
inquiry

References