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64020-33-3

5-Hexen-2-one, 1-phenyl- synthesis

11synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: dichloromethane / 20 °C
2: [4,4′-bis(1,1-dimethylethyl)-2,2′-bipyridine-κN1,κN1′]bis[3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl-κN]phenyl-κC]iridium hexafluorophosphate; 2-mesityl-6,7-dihydro-5H-pyrrolo[2,1-c][1,2,4]triazol-2-ium tetrafluoroborate; Cs2CO3 / acetonitrile / 20 °C / Inert atmosphere; Irradiation

References:

Bay, Anna V.;Cheong, Paul Ha-Yeon;Farah, Abdikani Omar;Fitzpatrick, Keegan P.;González-Montiel, Gisela A.;Scheidt, Karl A. [Angewandte Chemie - International Edition,2021,vol. 60,# 33,p. 17925 - 17931][Angew. Chem.,2021,vol. 133,# 33,p. 18069 - 18075]