(5-CHLORO-4-METHOXY-2-METHYLPHENYL)BORONIC ACID synthesis
- Product Name:(5-CHLORO-4-METHOXY-2-METHYLPHENYL)BORONIC ACID
- CAS Number:511295-09-3
- Molecular formula:C8H10BClO3
- Molecular Weight:200.43
615-74-7
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511295-09-3
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Yield:-
Steps:
Multi-step reaction with 3 steps
1.1: 89 percent / Br2 / CCl4 / 24 h / 20 °C
2.1: 76 percent / K2CO3 / acetone / 24 h / Heating
3.1: n-BuLi / tetrahydrofuran; hexane; diethyl ether / 0.08 h / -98 °C
3.2: B(OMe)3 / tetrahydrofuran; hexane; diethyl ether / 12 h / -98 - 20 °C
3.3: 65 percent / aq. HCl / tetrahydrofuran; hexane; diethyl ether / 20 °C
References:
Speicher, Andreas;Kolz, Juergen;Sambanje, Rufino Paulino [Synthesis,2002,# 17,p. 2503 - 2512]
179897-95-1
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511295-09-3
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$90.00/50mg
319473-24-0
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511295-09-3
32 suppliers
$90.00/50mg