5-CHLORO-1-OXO-1-(4-TRIFLUOROMETHYLPHENYL)PENTANE synthesis
- Product Name:5-CHLORO-1-OXO-1-(4-TRIFLUOROMETHYLPHENYL)PENTANE
- CAS Number:343968-74-1
- Molecular formula:C12H12ClF3O
- Molecular Weight:264.67
![Cyclopentanol, 1-[4-(trifluoromethyl)phenyl]-](/CAS/20210305/GIF/29480-11-3.gif)
29480-11-3
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343968-74-1
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Yield:-
Steps:
Multi-step reaction with 2 steps
1: dihydrogen peroxide; sulfuric acid / water; dichloromethane / 12 h / 0 - 25 °C / Schlenk technique; Inert atmosphere
2: copper diacetate; hydrogenchloride / 1-methyl-pyrrolidin-2-one; water / 2 h / 25 °C / Schlenk technique; Inert atmosphere; Sealed tube
References:
Bai, Ming;Duan, Xin-Hua;Guo, Li-Na;Liu, Shuai;Sun, Qing-Xin;Xu, Peng-Fei [Chemical Communications,2021,vol. 57,# 69,p. 8652 - 8655]
