5,7-DODECADIYNE-1,12-DIOL synthesis
- Product Name:5,7-DODECADIYNE-1,12-DIOL
- CAS Number:74602-32-7
- Molecular formula:C12H18O2
- Molecular Weight:194.27
100-72-1
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74602-32-7
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: pyridine; thionyl chloride / 3 h / 20 °C / Inert atmosphere
2: ammonia; Iron(III) nitrate nonahydrate; sodium / 4 h / Cooling
3: copper(l) chloride; oxygen; N,N,N,N,-tetramethylethylenediamine / acetone / 80 °C
References:
Kikuchi, Kohei;Tatewaki, Yoko;Okada, Shuji [Bulletin of the Chemical Society of Japan,2017,vol. 90,# 3,p. 298 - 305]
928-90-5
187 suppliers
$8.00/250mg
74602-32-7
31 suppliers
$141.00/1g
![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
1000210-73-0
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74602-32-7
31 suppliers
$141.00/1g