5-(2-METHYL-3-NITROPHENYL)-2-FURALDEHYDE synthesis
1synthesis methods
- Product Name:5-(2-METHYL-3-NITROPHENYL)-2-FURALDEHYDE
- CAS Number:725276-90-4
- Molecular formula:C12H9NO4
- Molecular Weight:231.2
Yield:-
Reaction Conditions:
Stage #1: 3-nitro-o-tolylaminewith tetrafluoroboric acid;sodium nitrite in water;
Stage #2: furfuralwith copper dichloride in acetone at 20; for 48 h;Further stages.;Meerwin arylation;
References:
Mugnaini, Claudia;Rajamaki, Suvi;Tintori, Cristina;Corelli, Federico;Massa, Silvio;Witvrouw, Myriam;Debyser, Zeger;Veljkovic, Veljko;Botta, Maurizio [Bioorganic and Medicinal Chemistry Letters,2007,vol. 17,# 19,p. 5370 - 5373]