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142779-83-7

4H-1,3-Dioxin-4-one, 5-iodo-2,2,6-trimethyl- synthesis

3synthesis methods
5394-63-8 Synthesis
2,2,6-Trimethyl-4H-1,3-dioxin-4-one

5394-63-8
227 suppliers
$19.00/25g

4H-1,3-Dioxin-4-one, 5-iodo-2,2,6-trimethyl-

142779-83-7
3 suppliers
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Yield:142779-83-7 86%

Reaction Conditions:

with N-iodo-succinimide;acetic anhydride at 20; for 8 h;Inert atmosphere;Darkness;

References:

Fuse, Shinichiro;Yoshida, Hayato;Oosumi, Kazuya;Takahashi, Takashi [European Journal of Organic Chemistry,2014,vol. 2014,# 22,p. 4854 - 4860] Location in patent:supporting information