2-Butylsulfanyl-thiocarbonylsulfanyl-propionic acid synthesis
- Product Name:2-Butylsulfanyl-thiocarbonylsulfanyl-propionic acid
- CAS Number:480436-46-2
- Molecular formula:C8H14O2S3
- Molecular Weight:238.39
75-15-0
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109-79-5
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598-72-1
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480436-46-2
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Yield:480436-46-2 81%
Reaction Conditions:
Stage #1: carbon disulfide;1-butanethiolwith sodium hydroxide in acetone at 20; for 0.5 h;
Stage #2: 2-Bromopropionic acidwith sodium hydroxide in acetone at 20; for 24 h;
References:
Ferguson, Christopher J.;Hughes, Robert J.;Nguyen, Duc;Pham, Binh T.T.;Gilbert, Robert G.;Serelis, Algirdas K.;Such, Christopher H.;Hawkett, Brian S. [Macromolecules,2005,vol. 38,# 6,p. 2191 - 2204]