3-[[4-[(2-chloro-4-nitrophenyl)azo]phenyl]ethylamino]propiononitrile synthesis
1synthesis methods
- Product Name:3-[[4-[(2-chloro-4-nitrophenyl)azo]phenyl]ethylamino]propiononitrile
- CAS Number:40880-51-1
- Molecular formula:C17H16ClN5O2
- Molecular Weight:357.8
2-Chloro-4-nitrobenzenamine diazo, and N-ethyl-N-cyanoethylaniline?coupling.
Yield:-
Reaction Conditions:
with sulfuric acid;sodium acetate;acetic acid;sodium nitrite1.) 10 deg C, 2.) 5 deg C, overnight;Yield given. Multistep reaction;
References:
Johri;Varshney [Journal of the Indian Chemical Society,1996,vol. 73,# 11,p. 629 - 630]