CARBAMIC ACID, (6-CHLORO-4-IODO-3-PYRIDINYL)-, 1,1-DIMETHYLETHYL ESTER synthesis
- Product Name:CARBAMIC ACID, (6-CHLORO-4-IODO-3-PYRIDINYL)-, 1,1-DIMETHYLETHYL ESTER
- CAS Number:400777-00-6
- Molecular formula:C10H12ClIN2O2
- Molecular Weight:354.57
4548-45-2
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400777-00-6
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Yield:-
Steps:
Multi-step reaction with 3 steps
1.1: tin(II) chloride dihdyrate; hydrogenchloride / 4 h / 0 - 20 °C
2.1: 1,4-dioxane / 45 h / Reflux; Inert atmosphere
3.1: N,N,N,N,-tetramethylethylenediamine; n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere
3.2: 20 °C / Inert atmosphere
References:
Boynton, Adam N.;Marcélis, Lionel;McConnell, Anna J.;Barton, Jacqueline K. [Inorganic Chemistry,2017,vol. 56,# 14,p. 8381 - 8389]
![5-[N-(TERT-BUTOXYCARBONYL)AMINO]-2-CHLOROPYRIDINE](/CAS/GIF/171178-45-3.gif)
171178-45-3
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400777-00-6
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5350-93-6
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400777-00-6
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24424-99-5
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$13.50/25G
400777-00-6
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