4-Nitropicolinaldehyde synthesis
- Product Name:4-Nitropicolinaldehyde
- CAS Number:108338-19-8
- Molecular formula:C6H4N2O3
- Molecular Weight:152.11
931-19-1
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108338-19-8
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$112.00/100mg
Yield:-
Steps:
Multi-step reaction with 4 steps
1: 95 percent / H2SO4, fuming HNO3 / 2 h / 100 - 105 °C
2: 18 percent / Heating
3: 74 percent / aq. NaOH / methanol / 1.5 h / Ambient temperature
4: 66 percent / DMSO, N,N'-dicyclohexylcarbodiimide, H3PO4 / 1.5 h / Ambient temperature
References:
Ashimori;Ono;Uchida;Ohtaki;Fukaya;Watanabe;Yokoyama [Chemical and Pharmaceutical Bulletin,1990,vol. 38,# 9,p. 2446 - 2458]
98197-88-7
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108338-19-8
49 suppliers
$112.00/100mg
5470-66-6
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$8.00/1g
108338-19-8
49 suppliers
$112.00/100mg
36625-64-6
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108338-19-8
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$112.00/100mg
131747-33-6
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108338-19-8
49 suppliers
$112.00/100mg