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124388-30-3

4-N-PENTYLPHENYLMAGNESIUM BROMIDE synthesis

2synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 71 percent / hydrazine hydrate, potassium hydroxide / bis-(2-hydroxy-ethyl) ether / 6 h / 130 - 180 °C
2: magnesium turnings / tetrahydrofuran

References:

Chan, L. K. M.;Gray, G. W.;Lacey, D.;Toyne, K. J. [Molecular Crystals and Liquid Crystals (1969-1991),1988,vol. 158,p. 209 - 240]

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