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ChemicalBook CAS DataBase List 4-N-HEXYLOXYBENZONITRILE
66052-06-0

4-N-HEXYLOXYBENZONITRILE synthesis

8synthesis methods
-

Yield:66052-06-0 100%

Reaction Conditions:

in potassium carbonate;

Steps:

34.A A.

A. 4-(Hexyloxy)Benzonitrile A solution of 4-cyanophenol (20 g, 168 mmol) in dimethylformamaide was treated with potassium carbonate (2 eq., 338 mmol, 47 g) and 1-bromohexane (1.1 eq., 185 mmol, 35 mL) and stirred at room temperature for 18 hours. The solid was filtered off and the solution was partitioned between ethyl acetate and 1 N HCl. The organic phase was washed with brine, dried over MgSO4, filtered and the solvent was removed to give compound 2 (45 g, >100%).

References:

US2002/137968,2002,A1

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