(4-ISOPROPOXY-PHENYL)-HYDRAZINE HYDROCHLORIDE synthesis
- Product Name:(4-ISOPROPOXY-PHENYL)-HYDRAZINE HYDROCHLORIDE
- CAS Number:104033-62-7
- Molecular formula:C9H15ClN2O
- Molecular Weight:202.68
7664-66-6
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Yield:104033-62-7 65%
Reaction Conditions:
Stage #1: 4-(isopropoxy)anilinewith hydrogenchloride in water at 0 - 20; for 0.416667 h;Inert atmosphere;
Stage #2: with sodium nitrite in water;Inert atmosphere;Cooling;
Stage #3: with tin(II) chloride dihdyrateInert atmosphere;
References:
Conlon, Ivie L.;Drennen, Brandon;Lanning, Maryanna E.;Hughes, Samuel;Rothhaas, Rebecca;Wilder, Paul T.;MacKerell, Alexander D.;Fletcher, Steven [ChemMedChem,2020,vol. 15,# 18,p. 1691 - 1698] Location in patent:supporting information
100-02-7
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26455-31-2
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104033-62-7
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