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ChemicalBook CAS DataBase List 4-(HYDROXYMETHYL)CYCLOHEXANONE
38580-68-6

4-(HYDROXYMETHYL)CYCLOHEXANONE synthesis

6synthesis methods
-

Yield:38580-68-6 73%

Reaction Conditions:

with NaBrO3;acetic acid in Ce

Steps:

5 EXAMPLE 5
EXAMPLE 5 To acetic acid in which Ce (IV)/PFCP (50 mg, 0.027 mmole) and 200 mg of NaBrO3 were dispersed and dissolved, 1.0 mmole of 1,10-undecane diol and 1.0 mmole of 4-hydroxymethyl cyclohexanol were added, respectively. The reaction mixture was heated for three hours at 55° C. and the product was purified with a column chromatography to yield 154 mg (82% yield) of 10-undecane-1-ol and 93 mg (73% yield) of 4-hydroxymethyl cyclohexanone.

References:

E. I. Du Pont de Nemours and Company US4617153, 1986, A

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