4-FLUORO-3-(TRIFLUOROMETHYL)BENZOYL CHLORIDE synthesis
- Product Name:4-FLUORO-3-(TRIFLUOROMETHYL)BENZOYL CHLORIDE
- CAS Number:67515-56-4
- Molecular formula:C8H3ClF4O
- Molecular Weight:226.56
67515-55-3
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$10.00/1g
67515-56-4
100 suppliers
$12.00/1g
Yield:-
Reaction Conditions:
with thionyl chloride in N,N-dimethyl-formamide;toluene
Steps:
2.a a
a 4-Fluoro-3-trifluoromethylbenzoyl Chloride 1.5 g of 4-fluoro-3-trifluoromethylbenzoic acid, 0.65 ml of thionyl chloride and two drops of DMF are heated under reflux for 12 h in 17 ml of toluene and the mixture is subsequently concentrated and used without further purification.
References:
Hoechst Aktiengesellschaft US6436999, 2002, B1