4-DIMETHYLAMINOSALICYLIC ACID synthesis
1synthesis methods
- Product Name:4-DIMETHYLAMINOSALICYLIC ACID
- CAS Number:23050-91-1
- Molecular formula:C9H11NO3
- Molecular Weight:181.19
Yield:23050-91-1 62%
Reaction Conditions:
Stage #1: 3-Dimethylaminophenolwith Mesitol;sodium hydride in mineral oil at 100; for 0.0833333 h;Glovebox;
Stage #2: carbon dioxide in mineral oil at 185; under 760.051 Torr; for 2 h;
References:
Luo, Junfei;Preciado, Sara;Xie, Pan;Larrosa, Igor [Chemistry - A European Journal,2016,vol. 22,# 20,p. 6798 - 6802] Location in patent:supporting information