(4-BROMO-3,5-DIMETHYL)PHENYL BENZYL ETHER synthesis
- Product Name:(4-BROMO-3,5-DIMETHYL)PHENYL BENZYL ETHER
- CAS Number:95741-44-9
- Molecular formula:C15H15BrO
- Molecular Weight:291.18
7463-51-6
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Yield:95741-44-9 97%
Reaction Conditions:
Stage #1: 4-bromo-3,5-dimethylphenolwith sodium hydroxide in methanol at 0; for 2 h;Metallation;
Stage #2: benzyl chloride in 1,2-dimethoxyethane at 35; for 24 h;Etherification;
References:
Tang, Xuejun;Soloshonok, Vadim A.;Hruby, Victor J. [Tetrahedron Asymmetry,2000,vol. 11,# 14,p. 2917 - 2925]
