4-BROMO-2,3-DIHYDRO-1H-INDEN-1-OL synthesis
- Product Name:4-BROMO-2,3-DIHYDRO-1H-INDEN-1-OL
- CAS Number:16657-10-6
- Molecular formula:C9H9BrO
- Molecular Weight:213.07
3433-80-5
314 suppliers
$10.00/1g
16657-10-6
67 suppliers
$25.00/250mg
Yield:-
Steps:
Multi-step reaction with 6 steps
1: 64 percent / NaOC2H5 / 3.5 h / Heating
2: 89 percent / KOH / acetic acid; H2O; tetrahydrofuran / 12 h / 25 °C
3: 81 percent / 165 °C
4: thionyl chloride / 0.75 h / Heating
5: 93 percent / AlCl3 / CS2 / 3 h / Heating
6: 98 percent / NaBH4 / ethanol / 2 h / 25 °C
References:
Adamczyk, Maciej;Watt, David S.;Netzel, Daniel A. [Journal of Organic Chemistry,1984,vol. 49,# 22,p. 4226 - 4237]
15115-60-3
330 suppliers
$5.00/1g
16657-10-6
67 suppliers
$25.00/250mg
15115-58-9
198 suppliers
$14.00/1g
16657-10-6
67 suppliers
$25.00/250mg
90725-40-9
4 suppliers
inquiry
16657-10-6
67 suppliers
$25.00/250mg
![Propanedioic acid, [(2-bromophenyl)methyl]-, diethyl ester](/CAS/20180601/GIF/66192-11-8.gif)
66192-11-8
11 suppliers
inquiry
16657-10-6
67 suppliers
$25.00/250mg