4-AMINO-N-(2-HYDROXYETHYL)BENZENESULFONAMIDE synthesis
- Product Name:4-AMINO-N-(2-HYDROXYETHYL)BENZENESULFONAMIDE
- CAS Number:4862-94-6
- Molecular formula:C8H12N2O3S
- Molecular Weight:216.26
18226-05-6
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4862-94-6
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Yield:4862-94-6 98.7%
Reaction Conditions:
with palladium 10% on activated carbon;hydrogen in methanol at 20; for 2 h;
Steps:
23
Compound 23a (150 mg, 0.61 mmol) was dissolved in methanol (5 mL), Pd/C (30 mg, 10% w/w) was added, and the resulting reaction solution was stirred at room temperature for 2 hours under a hydrogen atmosphere. The reaction solution was filtered through Celite, and the filtrate was concentrated under reduced pressure to obtain a white solid compound 23b (130 mg, yield: 98.7%).
References:
CN112707902,2021,A Location in patent:Paragraph 0159-0160; 0162
![N-(4-[[(2-HYDROXYETHYL)AMINO]SULFONYL]PHENYL)ACETAMIDE](/CAS/GIF/20535-76-6.gif)
20535-76-6
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4862-94-6
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121-60-8
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4862-94-6
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98-74-8
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4862-94-6
32 suppliers
$75.00/250mg