4-ACETOXY-N,N-DIMETHYLTRYPTAMINE synthesis

6synthesis methods

Product Name:4-ACETOXY-N,N-DIMETHYLTRYPTAMINE
CAS Number:92292-84-7
Molecular formula:C14H18N2O2
Molecular Weight:246.3

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Yield:-

Steps:

Multi-step reaction with 4 steps
1: diethyl ether / 3 h / 5 - 10 °C
2: diethyl ether; CH₂Cl₂ / 6 h
3: 94.8 percent / LiAlH₄ / tetrahydrofuran; dioxane / 1.) 4 h, 2.) reflux, 20 h
4: H₂, AcONa / 10 percent Pd/C / benzene / 4 h / 3102.89 Torr

References:

Nichols, David E.;Frescas, Stewart [Synthesis,1999,# 6,p. 935 - 938]

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References

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References

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References

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