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837365-03-4

(4,6-DICHLORO-PYRIDIN-2-YL)-HYDRAZINE synthesis

4synthesis methods
Pyridine, 2,4,6-trichloro-3-(trimethylsilyl)-

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(4,6-DICHLORO-PYRIDIN-2-YL)-HYDRAZINE

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-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: H2NNH2*H2O / tetrahydrofuran / 20 h / 50 °C
2: 6.41 g / tetrabutylammonium fluoride trihydrate / tetrahydrofuran / 2 h / 25 °C

References:

Schlosser, Manfred;Bobbio, Carla;Rausis, Thierry [Journal of Organic Chemistry,2005,vol. 70,# 7,p. 2494 - 2502]