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23459-13-4

4,4-DIMETHYL-3-OXO-PENTANAL synthesis

2synthesis methods
-

Yield:23459-13-4 61%

Reaction Conditions:

with ethanol;sodium hydride in tert-butyl methyl ether at 20; for 1.66667 h;Inert atmosphere;Reflux;Claisen condensation;

References:

Bertogg, Andreas;Hintermann, Lukas;Huber, Dominique P.;Perseghini, Mauro;Sanna, Maria;Togni, Antonio [Helvetica Chimica Acta,2012,vol. 95,# 3,p. 353 - 403] Location in patent:experimental part

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