4-(2-DIMETHYLAMINOETHYL)PYRIDINE synthesis
- Product Name:4-(2-DIMETHYLAMINOETHYL)PYRIDINE
- CAS Number:38223-06-2
- Molecular formula:C9H14N2
- Molecular Weight:150.22
100-43-6
150 suppliers
$26.19/5ml
124-40-3
520 suppliers
$18.00/100ml
38223-06-2
13 suppliers
inquiry
Yield:38223-06-2 90%
Reaction Conditions:
with NPs-Fe3O4-DE-bmim3PW in dichloromethane at 20; for 2 h;
Steps:
N,N-dimethyl-2-(pyridin-4-yl)ethanamine (3b)
4-vinylpyridine (0.53 g, 5 mmol, 1 equiv.) and dimethylamine (0.23 g, 5 mmol, 1 equiv.) were added to a mixture of NPs-Fe3O4-DE-bmim3PW (catalyst I, 3 mol%) in 5 mL of dichloromethane and stirred at room temperature for 2 hours. Purification and separation of the product is similar to the described procedure for compound 1a. N,N-dimethyl-2-(pyridin-4-yl)ethanamine (3b) was synthesised as a viscous yellow oil (0.67 g, 90%).
References:
Ghasemi, Mohammad Hadi;Kowsari, Elaheh;Shafiee, Abbas [Tetrahedron Letters,2016,vol. 57,# 10,p. 1150 - 1153] Location in patent:supporting information
100-43-6
150 suppliers
$26.19/5ml
38223-06-2
13 suppliers
inquiry
10445-91-7
39 suppliers
inquiry
38223-06-2
13 suppliers
inquiry