6-METHOXY-1,2,3,4-TETRAHYDRO-NAPHTHALEN-1-YLAMINE HYDROCHLORIDE synthesis
- Product Name:6-METHOXY-1,2,3,4-TETRAHYDRO-NAPHTHALEN-1-YLAMINE HYDROCHLORIDE
- CAS Number:39226-88-5
- Molecular formula:C11H16ClNO
- Molecular Weight:213.7
54951-36-9
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39226-88-5
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Yield:39226-88-5 2.13 g
Reaction Conditions:
with hydrogenchloride;palladium 10% on activated carbon;hydrogen in ethanol; under 760.051 Torr;
Steps:
96
Second step, 6-methoxy-1,2,3,4-tetrahydro-1-tetralone oxime (1.87 g) and concentrated HCl (4 ml) in EtOH (50 ml) was subjected to hydrogenation at atmospheric pressure in the presence of 10% Pd/C (150 mg). The reaction solution was filtered and the filtrate was concentrated. The residue was suspended in EtOAc, and the suspension was filtered to yield (+/-)-6-methoxy-1,2,3,4-tetrahydro-naphthalene-1-ylamine hydrochloride (2.13 g) as a white solid.
References:
US2013/45942,2013,A1 Location in patent:Paragraph 0383
52373-02-1
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39226-88-5
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1730-48-9
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39226-88-5
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120342-64-5
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1078-19-9
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39226-88-5
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$60.00/50mg