ChemicalBook CAS DataBase List (αR,βS)-β-[[(1,1-DiMethylethoxy)carbonyl]aMino]-α-hydroxy-4-(phenylMethoxy)-benzenepropanoic Acid Ethyl Ester

(αR,βS)-β-[[(1,1-DiMethylethoxy)carbonyl]aMino]-α-hydroxy-4-(phenylMethoxy)-benzenepropanoic Acid Ethyl Ester synthesis

2synthesis methods

Product Name:(αR,βS)-β-[[(1,1-DiMethylethoxy)carbonyl]aMino]-α-hydroxy-4-(phenylMethoxy)-benzenepropanoic Acid Ethyl Ester
CAS Number:382596-26-1
Molecular formula:C23H29NO6
Molecular Weight:415.4795

4397-53-9
325 suppliers
$8.00/10g

(αR,βS)-β-[[(1,1-DiMethylethoxy)carbonyl]aMino]-α-hydroxy-4-(phenylMethoxy)-benzenepropanoic Acid Ethyl Ester

382596-26-1
6 suppliers
$1410.00/25mg

Yield:-

Steps:

Multi-step reaction with 3 steps
1.1: 90 percent / CH₂Cl₂ / 24 h / 20 °C
2.1: K₂[OsO₂(OH)4]; LiOH*H₂O; (DHQ)2PHAL / 2-methyl-propan-2-ol; H₂O; acetonitrile / 24 h / 0 - 5 °C
2.2: HCl / ethanol / 4 h / 90 °C
3.1: 23 g / NaHCO₃ / tetrahydrofuran / 5 h / 20 °C

References:

Reddy, S. Hari Krishna;Lee, Stephen;Datta, Apurba;Georg, Gunda I. [Journal of Organic Chemistry,2001,vol. 66,# 24,p. 8211 - 8214]

104315-07-3
24 suppliers
$155.00/100mg

382596-26-1
6 suppliers
$1410.00/25mg

References

(αR,βS)-β-[[(1,1-DiMethylethoxy)carbonyl]aMino]-α-hydroxy-4-(phenylMethoxy)-benzenepropanoic Acid Ethyl Ester Related Search:

Epothilone B 6-CHLORO-4-CHLOROMETHYL-7-HYDROXY-CHROMEN-2-ONE (4S,5R)-2,2-DiMethyl-4-[4-(phenylMethoxy)phenyl]-N-DiMethylethoxycarbonyl-3,5-oxazolidinecarboxylic Acid Ethyl Ester (3S,6R,7S,12Z,15S,16E)-3,7-Bis-{[tert-butyl(dimethyl)silyl]oxy}-15-hydroxy-4,4,6,8,12,16-hexamethyl-17-(2-methyl-1,3-thiazol-4-yl)-5-oxoheptadeca-12,16-dienoic Acid Methyl (2R,3S)-3-(benzoylamino)-2-hydroxy-3-phenylpropanoate (4S,5R)-2,2-DiMethyl-4-[4-(phenylMethoxy)phenyl]-3,5-oxazolidinedicarboxylic Acid 3-(1,1-DiMethylethyl) Ester 2-Bromobenzene-1,3-dialdehyde 4-[(1E,3S,5Z,8R/S,10S)-3,11-Bis-{[tert-butyl(dimethyl)silyl]oxy}-2,6,10-trimethyl-8-(phenylsulfonyl)undeca-1,5-dienyl]-2-methyl-1,3-thiazole Docetaxel 2’-tert-Butylsimethylsilyl Ether (4S,7R,8S,9S,13Z,16S)-4,8-Bis-{[tert-butyl(dimethyl)silyl]oxy}-5,5,7,9,13-pentamethyl-16-[(E)-1-methyl-2-(2-methyl-1,3-thiazol-4-yl)ethenyl]oxocyclohexadec-13-ene-2,6-dione

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(αR,βS)-β-[[(1,1-DiMethylethoxy)carbonyl]aMino]-α-hydroxy-4-(phenylMethoxy)-benzenepropanoic Acid Ethyl Ester synthesis

(αR,βS)-β-[[(1,1-DiMethylethoxy)carbonyl]aMino]-α-hydroxy-4-(phenylMethoxy)-benzenepropanoic Acid Ethyl Ester Related Search: