TRANS-1-(2-(4-METHOXYPHENYL)ETHYNYL)-4-(4-PENTYLCYCLOHEXYL)BENZENE synthesis

1synthesis methods

Product Name:TRANS-1-(2-(4-METHOXYPHENYL)ETHYNYL)-4-(4-PENTYLCYCLOHEXYL)BENZENE
CAS Number:372983-17-0
Molecular formula:C26H32O
Molecular Weight:360.53

79832-89-6 Synthesis

1-Bromo-4-(trans-4-pentylcyclohexyl)benzene

79832-89-6
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768-60-5
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TRANS-1-(2-(4-METHOXYPHENYL)ETHYNYL)-4-(4-PENTYLCYCLOHEXYL)BENZENE

372983-17-0
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Yield:372983-17-0 71%

Reaction Conditions:

with Ph₂P(CH₂CH₂O)22CH₃;triethylamine;palladium dichloride in water at 80; for 8 h;Inert atmosphere;Sonogashira coupling;

References:

Liu, Ning;Liu, Chun;Xu, Qiang;Jin, Zilin [European Journal of Organic Chemistry,2011,# 23,p. 4422 - 4428] Location in patent:supporting information; experimental part

TRANS-1-(2-(4-METHOXYPHENYL)ETHYNYL)-4-(4-PENTYLCYCLOHEXYL)BENZENE Related Search:

1-(4-N-BUTYLPHENYL)-2-(4-METHOXYPHENYL)ACETYLENE 1-(4-METHOXYPHENYL)-2-(4-N-PROPYLPHENYL)ACETYLENE P-ETHYNYLOCTYLBENZENE 1-ETHYNYL-4-HEPTYLBENZENE