(1S,2R,4R)-N-BOC-1-AMINO-2-HYDROXYCYCLOPENTANE-4-CARBOXYLIC ACID METHYL ESTER synthesis
- Product Name:(1S,2R,4R)-N-BOC-1-AMINO-2-HYDROXYCYCLOPENTANE-4-CARBOXYLIC ACID METHYL ESTER
- CAS Number:321744-23-4
- Molecular formula:C12H21NO5
- Molecular Weight:259.3
![(1R-4S)-4-[[(1,1-dimethylethoxy)carbonyl]amino]- 2-Cyclopentene-1-carboxylic acid methyl ester](/CAS2/GIF/251326-99-5.gif)
251326-99-5
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321744-23-4
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Yield:-
Steps:
Multi-step reaction with 4 steps
1.1: N-bromosuccinimide / tetrahydrofuran; H2O / 17 h / 20 °C
2.1: KOH / H2O; methanol / 48 h / 90 °C
2.2: tetrahydrofuran; H2O / 14 h / 20 °C / pH 10.5
3.1: H2 / Pd/C / methanol / 18 h / 20 °C / 1500.15 Torr
4.1: triethylamine / methanol / 5 - 20 °C
References:
Lloyd, Richard C.;Lloyd, Michael C.;Smith, Mark E. B.;Holt, Karen E.;Swift, Jonathan P.;Keene, Philip A.;Taylor, Stephen J. C.;McCague, Raymond [Tetrahedron,2004,vol. 60,# 3,p. 717 - 728]
![1-Cyclopentene-1-carboxylic acid, 4-[[(1,1-dimethylethoxy)carbonyl]amino]-3-hydroxy-, (3R,4S)-](/CAS/20210305/GIF/329910-36-3.gif)
329910-36-3
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321744-23-4
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![Cyclopentanecarboxylic acid, 3-[[(1,1-dimethylethoxy)carbonyl]amino]-4-hydroxy-, (1R,3S,4R)-](/CAS/20210305/GIF/927870-60-8.gif)
24424-99-5
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321744-23-4
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329910-34-1
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321744-23-4
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