3-Tert-butyl-5-methylsalicylicacid synthesis

4synthesis methods

Product Name:3-Tert-butyl-5-methylsalicylicacid
CAS Number:23050-96-6
Molecular formula:C12H16O3
Molecular Weight:208.25

2409-55-4 Synthesis

2409-55-4
285 suppliers
$7.00/25g

23050-96-6
8 suppliers
$55.00/250mg

Yield:-

Steps:

Multi-step reaction with 3 steps
1: 84 percent / p-toluenesulfonic acid, 4A molecular sieves / CH₂Cl₂ / 72 h / Heating
2: 1.) TMEDA, n-BuLi / 1.) Et₂O, from -50 deg C to -5 deg C, 4 h, 2.) Et₂O, RT, overnight
3: glacial acetic acid / 1 h / Heating

References:

Katritzky;Lang;Lan [Synthetic Communications,1993,vol. 23,# 8,p. 1175 - 1182]

1H-Indene-1,3(2H)-dione, 2-(3-(1,1-dimethylethyl)-2-hydroxy-5-methylphenyl)-2-hydroxy-

71313-39-8
0 suppliers
inquiry

23050-96-6
8 suppliers
$55.00/250mg

References

1H-Isoindol-1-one, 3-[3-(1,1-dimethylethyl)-2-hydroxy-5-methylbenzoyl]-2,3-dihydro-2-(4-methylphenyl)-

95646-21-2
0 suppliers
inquiry

23050-96-6
8 suppliers
$55.00/250mg

References

Benzene, 2-(1,1-dimethylethyl)-1-(methoxymethoxy)-4-methyl-

150094-87-4
1 suppliers
inquiry

23050-96-6
8 suppliers
$55.00/250mg

References

3-Tert-butyl-5-methylsalicylicacid Related Search:

3,5-Bis-tert-butylsalicylic acid