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130722-42-8

3-Oxepanone synthesis

3synthesis methods
3-Oxepanone

130722-42-8
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3-Oxepanecarboxylic acid, 3-amino-, methyl ester

1452228-32-8
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Yield:-

Steps:

Multi-step reaction with 4 steps
1: methanol; water / 16 h / 20 °C
2: hydrogenchloride; acetic acid; water / 24 h / Reflux
3: hydrogenchloride / Reflux
4: hydrogen; palladium 10% on activated carbon / methanol / 30 °C / 2585.81 Torr

References:

US2013/225593,2013,A1

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