3-Methoxybenzylamine synthesis
- Product Name:3-Methoxybenzylamine
- CAS Number:5071-96-5
- Molecular formula:C8H11NO
- Molecular Weight:137.18
1527-89-5
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5071-96-5
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Yield:5071-96-5 95%
Reaction Conditions:
with ammonia borane in methanol at 50; for 12 h;Inert atmosphere;
Steps:
8
Add PdNPore (2.7mg, 5mol%) catalyst into the mesoporous reactorAnd ammonia borane complex (30.86mg, 1mmol),Add methanol (3mL) under nitrogen,Add the substrate m-methoxybenzonitrile (58.5mg, 0.5mmol),Put it in an oil bath and react at 50 for 12h,After separation and purification by column chromatography (silica gel, 200-300 mesh; the developing solvent is ethyl acetate: methanol = 2:1),Obtained 65.4 mg of m-methoxybenzylamine,The yield was 95%.
References:
CN112851521,2021,A Location in patent:Paragraph 0077-0080
591-31-1
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5071-96-5
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5813-86-5
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5071-96-5
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38489-80-4
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5071-96-5
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![Carbamic acid, N-[(3-methoxyphenyl)methyl]-, 1,1-dimethylethyl ester](/CAS/20210111/GIF/153903-22-1.gif)
153903-22-1
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5071-96-5
255 suppliers
$5.00/1g