3'-Methanesulfonyl-biphenyl-4-carboxylic acid synthesis
- Product Name:3'-Methanesulfonyl-biphenyl-4-carboxylic acid
- CAS Number:16734-97-7
- Molecular formula:C14H12O4S
- Molecular Weight:276.31
33733-73-2
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: potassium phosphate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2 / N,N-dimethyl-formamide / 16 h / 80 °C / Inert atmosphere
2: potassium peroxymonosulfate sulfate / methanol; water / 16 h / 25 °C
3: hydrogenchloride; lithium hydroxide monohydrate / methanol; tetrahydrofuran; water / 16 h / 25 °C
References:
WO2020/198478,2020,A1
![[1,1'-Biphenyl]-4-carboxylic acid, 3'-(methylsulfonyl)-, methyl ester](/CAS/20210305/GIF/867256-61-9.gif)
867256-61-9
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99768-12-4
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