ChemicalBook CAS DataBase List 3-(DIMETHYLAMINO)-1-PHENYL-2-BUTEN-1-ONE

3-(DIMETHYLAMINO)-1-PHENYL-2-BUTEN-1-ONE synthesis

6synthesis methods

Product Name:3-(DIMETHYLAMINO)-1-PHENYL-2-BUTEN-1-ONE
CAS Number:34523-87-0
Molecular formula:C12H15NO
Molecular Weight:189.25

18871-66-4 Synthesis

18871-66-4
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$11.00/1g

98-86-2 Synthesis

98-86-2
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$9.00/5g

3-(DIMETHYLAMINO)-1-PHENYL-2-BUTEN-1-ONE

34523-87-0
10 suppliers
$45.00/50mg

Yield:-

Reaction Conditions:

for 20 h;Reflux;

Steps:

1. General Procedure for the Synthesis of 3-(Dimethylamino)-1-arylprop-2-en-1-ones 1a-l

General procedure: A solution of substituted acetophenone (2 nmol) in N,N-dimethylformamide dimethyl acetal or N,N-dimethylacetamide dimethyl acetal (10 mL) was refluxed for 20 h during which time some methanol was formed and removed through a reflux condenser. After cooling, the precipitate was collected by suction to give compounds 1.

References:

Dou, Guolan;Xu, Pan;Li, Qiang;Xi, Yukun;Huang, Zhibin;Shi, Daqing [Molecules,2013,vol. 18,# 11,p. 13645 - 13653]